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Butyl Paraben Chemicals

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Creating a niche of Butyl Paraben Chemicals such as Butyl Paraben B.P., Butyl Paraben U.S.P. and Butyl Paraben N.F. at its best, with utmost quality.

Butyl Paraben B.P.

The chemical name for Butyl Paraben B.P is Butyl 4-Hydroxy Benzoate. The molecular formula is C11H14O3 with the molecular weight of 194.2and CAS Number 94-26-8. The shelf life of the chemical is 5 years and is available in packing of 25 Kg and 20 Kg (4 x 5 kg). It is recommended to store the product in tightly closed containers. It is widely used as an Antimicrobial Preservative.

 

The various specifications of the chemical are:

 

  • Character: A white or almost white powder, crystalline powder or colorless crystals, very slightly soluble in water, freely soluble in alcohol and in methanol.
  • Identification:

-First identification: A, B.

-Second identification: A, C, D.

  • Test A: Melts between 68°C and 71°C.
  • Test B: The infrared absorption spectrum is concordant with the reference spectrum of Ethyl paraben or with the spectrum obtained from Ethyl paraben CRS.
  • Test C: Examine the chromatograms obtained in the test for related substances. The principle spot in the chromatogram obtained with test solution (b) is similar in position and size to the principle spot in the chromatogram obtained with reference solution (b).
  • Test D: To about 10 mg in a test tube add 1 ml of sodium carbonate solution,heat to boiling for 30 seconds and cool (solution A) to a further 10mg in a test tube add 1 ml of sodium carbonate solution, the substance partly dissolves (solution B). Add at the same time to each of solutions A and B 5ml of aminopyrazolone solution R and 1 ml of potassium ferricyanide solution R and mix. Solution B is yellow to orange brown. Solution A is orange to Red and the colour is clearly more intense than any similar colour that may be obtained with solution B.
  • Appearance of solution: A 10% w/v solution in ethanol (95%) is clear and not more intensely coloured than reference solution prepared by mixing 1.5 ml ferric chloride colorimetric solution, 0.8 ml cobaltous chloride colorimetric solution, 0.2 ml cupric sulphate colorimetric solution and 97.5 ml of 1% w/v HCl solution.
  • Acidity: Dissolve 1.0 g in sufficient ethanol (95%) to produce 10 ml. To 2 ml of the solution add 3 ml of alcohol R, 5 ml of carbon dioxide-free water and 0.1 ml of bromocresol green solution R. Not more than 0.1ml of 0.1M sodium hydroxide is required to change the colour of the solution to blue.
  • Related Substances: Not more than 0.5 %
  • Sulphated ash: Not more than 0.1 %.
  • Assay w/w: 99.0 to 100.5 %.

Butyl Paraben B.P.

Butyl Paraben U.S.P.

Butyl Paraben U.S.P.

The chemical name for Butyl Paraben U.S.P.is Butyl 4-Hydroxy Benzoate. The molecular formula is C11H14O3 with the molecular weight of 194.2and CAS Number 94-26-8. The shelf life of the chemical is 5 years and is available in packing of 25 Kg and 20 Kg (4 x 5 kg). It is recommended to store the product in tightly closed containers. It is widely used as an Antimicrobial Preservative.

 

The various specifications of the chemical are:

 

NO.

Test

Specifications

1

 Description &  solubility

Small, colourless crystals or white powder.

  2.

 Solubility

Slightly soluble in water and in glycerin, freely soluble in acetone, in alcohol, in ether and in propylene glycol.

3

 Identification

A. Infrared Absorption <197M>  

4

 Melting Range,   °C

Between 68°Cand 72°C

5

 Acidity

Dissolve 1.0 g in sufficient ethanol (96%) to produce 10 ml.  To 2 ml of the solution add 3 ml of ethanol (96%), 5 ml of carbon dioxide-free water and 0.1 ml of Bromocresol green solution .Not more than 0.1 ml of 0.1 N sodium hydroxide VS is required to change the colour of the solution to blue.

6

 Loss on       drying,w/w

Not more than 0.5 %.

7

 Residue on  ignition

Not more than 0.05 %.

8

 Organic volatile  impurities

Method IV <467>: meets the requirements.

9

 Assay, w/w

99.0 % - 100.5 %

Butyl Paraben N.F.

The chemical name for Butyl Paraben U.S.P.is Butyl Paraben N.F. The molecular formula is C11H14O3 with the molecular weight of 194.2and CAS Number 94-26-8. The shelf life of the chemical is 5 years and is available in packing of 25 Kg and 20 Kg (4 x 5 kg). It is recommended to store the product in tightly closed containers. It is widely used as an Antimicrobial Preservative.

 

The various specifications of the chemical are:

 

NO.

Test

Specifications

1

 Description &  solubility

Small, colourless crystals or white powder. Very slightly soluble in water and in glycerine: freely soluble in acetone, in alcohol, in ether and in propylene glycol.

2

 Identification

B.Infrared Absorption <197M>

3

 Melting Range

Between 68°C and 72°C

4

 Organic volatile  impurities

Method IV <467>: meets the requirements.

5

 Acidity

Heat 0.75 g in 15 mL of water at80o for 1 minute, cool, and filter: the filtrate is neutral or acid to litmus. To 10 mL of the filtrate add 0.20 mLof 0.1 N sodium hydroxide and 2 drop of methyl red TS : the solution is yellow.

6

 Loss on drying

Dry it over silica gel for 5 hours: it loses not more than 0.5 % of its weight.

Butyl Paraben N.F.


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