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X Ray Diffractometer

Pioneers in the industry, we offer Rigaku Ultima IV X Ray Diffractometer, Rigaku Smart Lab X Ray Diffractometer, Rigaku Automate II Stress Analyzers and Rigaku SmartSite RS Stress Analyzers from India.

Rigaku Ultima IV X Ray Diffractometer
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BrandRigaku
ModelUltima IV
Maximum Rated Output3 kW
Rated Tube Voltage20-60 kV
Rated Tube Current2-60 mA
TargetCu (others optional)
Focus Size0.4 x 12 mm (others optional)
Goniometer radius285 mm
Minimum Step Size0.0001 Degree
Divergence SlitFixed or Automatic Variable
Scattering SlitFixed or Automatic Variable
Receiving SlitFixed or Automatic Variable
Optics AlignmentAutomatic alignment of tube height, goniometer, optics and detector
MonochromatorDual position graphite diffracted beam monochromator for Cu (others optional)
DetectorScintillation counter (others optional)
H x W x D1600 x 1100 x 800 mm
Sample Height1050 mm

The Ultima IV represents the state-of-the-art in multipurpose X-ray diffraction (XRD) systems. Incorporating Rigaku's patented cross beam optics (CBO) technology for permanently mounted, permanently aligned and user-selectable parallel and focusing geometries, the Ultima IV X-ray diffractometer can perform many different measurements fast.

 

Engineered for Performance
With a multipurpose diffractometer, performance is measured by not only how fast you perform an experiment but also how fast you can switch between different types of experiments. Individual experiments are optimized with accessories like the D/teX Ultra high-speed position sensitive detector system, but the speed between experiments is radically improved with the combination of the automated alignment and CBO.

Designed for Flexibility

The Ultima IV is the only XRD system on the market today that incorporates fully automatic alignment. When coupled with CBO and the in-plane arm, the automatic alignment capability makes the Ultima IV X-ray diffractometer the most flexible system available for multipurpose applications.


Functionality Redefined

In the Ultima IV XRD system, CBO technology eliminates time spent switching geometries, enables everyday users to run both sets of experiments without the need to reconfigure the system, and reduces wear and possible optic damage associated with the recurrent switching process. CBO and automatic alignment combine for the ultimate in functionality for micro-crystalline diffraction, thin-film diffraction, small angle scattering, and in-plane scattering.

 

Features:

  • Full automated alignment under computer control.
  • Optional in-plane diffraction arm for in-plane measurements without reconfiguration.
  • Focusing and parallel beam geometries without reconfiguration.
  • SAXS capabilities.
  • Optional D/teX Ultra high-speed, position-sensitive detector system


Other details:

  • Scanning mode: θs/θd coupled or θs, θd independent
  • 2θ measuring range: -3 to 162° (maximum)



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Rigaku Smart Lab X Ray Diffractometer
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BrandRigaku
ModelSmartLab
X ray Generator3 kW for sealed x-ray tube, 9 kW for PhotonMax rotating anode
Tube Voltage Variable Range20-60 kV(3 kW for sealed x-ray tube), 20-45 kV(9 kW for PhotonMax rotating anode)
Tube Current Variable Range2-50 mA(3 kW for sealed x-ray tube), 10-200 mA( 9 kW for PhotonMax rotating anode)
Enclosure Dimension1300x1300x1880 mm, 51.2x51.2x74 inch(WxDxH)
Ground ResistanceLess than or equal to 100 ohm
Weight~750 kg, 1653 lb(3 kW for sealed x-ray tube), ~850 kg, 1874 lb(9 kW for PhotonMax rotating anode)

Rigaku SmartLab is the newest and most novel high-resolution X-ray diffractometer (XRD) available today. Perhaps its most novel feature is the new SmartLab Studio II software, which provides the user with an intelligent User Guidance expert system functionality that guides the operator through the intricacies of each experiment. It is like having an expert standing by your side.

 

Engineered for Performance

This new X-ray diffraction system features the PhotonMax high-flux 9 kW rotating anode X-ray source coupled with a HyPix-3000 high-energy-resolution 2D multidimensional semiconductor detector that supports 0D, 1D and 2D measure­ment modes, allowing all applications to be handled with a single detector, eliminating the inconvenience of preparing and switching individual detectors for different applications. The HyPix-3000 detector can be used to obtain 2D powder diffraction patterns, which can be processed to deliver superior qualitative analysis by using all the 2D pattern information. The system incorporates a high-resolution θ/θ closed loop goniometer drive system with an available in-plane diffraction arm. The system’s new Cross-Beam-Optics (CBO) family feature fully automated switchable reflection and transmission optics (CBO-Auto).

 

Designed for Flexibility

Coupling a computer controlled alignment system with a fully automated optical system, and the User Guidance functionality within the SmartLab Studio II software, makes it easy to switch between hardware modes, ensuring that your hardware complexity is never holding back your research.

 

Functionality Redefined

Whether you are working with thin films, nanomaterials, powders, or liquids the SmartLab will give you the XRD functionality to make the measurements you want to make when you want to make them. The equipment accepts powder, liquid, films, and even textile samples and allows mapping measurements within suitable samples. Operando (a.k.a., real time in-situ) measurements can be performed with the new Rigaku SmartLab Studio II software suite, which is an integrated software platform incorporating all functions from measurement to analysis. The system also features robust security and validation protocols to ensure that any technology component - software or hardware - fulfills its purpose within regulatory guidelines, including 21 CFR Part 11, establishing the US EDA regulations governing electronic records and electronic signatures (ER/ES).

 

Features:

  • Available in-plane arm (5-axis goniometer)
  • Highest flux X-ray source: PhotonMax
  • HyPix-3000 high energy resolution 2D HPAD detector
  • New CBO family, with fully automated beam switchable CBO-Auto and high-resolution micro area CBO-μ
  • Operando measurements with SmartLab Studio II software
  • Multi-year component warranty contributes to the low cost of ownership

Power Supply:
  • Three phases AC200V, 50/60 Hz, 30 A or single phase AC200-230V, 50/60 Hz, 40A(3 kW for sealed x-ray tube)
  • Three phases AC200V, 50/60 Hz, 60 A (9 kW for PhotoMax rotating anode)

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Rigaku Automate II Stress Analyzers
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BrandRigaku
ModelAutoMATE II
Maximum Power3 kW (Tube voltage 20 - 50 kV, Tube current 2 - 50 mA)
Stability+/-0.03 % (Power fluctuation within +/-10%)
DistanceX-ray source - sample 265 mm, Sample - detector 210 mm
X ray ShutterRotary Shutter
CCD Camera(Magnification) x22 to x135 (Field of vision 6 mm to 1 mm), Focal distance(90 mm)
DimensionOne dimension (Semiconductor system)
Number of Channels1024 channel
Maximum Counting Rate1 x 106 cps/ch x 1024 ch (Total 1 Gcps/all)
Window Area76.8 mm x 10 mm
Size135 mm (W) x 95 mm (D) x 100 mm (H)
Weight1.4 kg
Cooling SystemAir-cooled water chiller
Cooling Capacity2 kW
Cooling Temperature Range15 Degree C to 25 Degree C
PCDesktop Personal Computer
OSWindows 7 Professional (32 bit)
Display19" TFT
PrinterInk jet color printer
Computer RackVertical Type

Residual stress may be created during the manufacturing process of a material, or it may accumulate in a structure over many years in operation.

 

With the AutoMATE II, you now have the best of both worlds. Large and heavy parts (30 kg with standard manual Z stage; 20 kg with optional automated XYZ stage) can be measured with high accuracy. This is possible because the X-ray source and detector arm are mounted on a highly accurate two-axis goniometer that can position them relative to the measurement site and perform scans with an accuracy of 0.1 microns when using the automated XYZ stage.

 

The detector used in the AutoMATE II is the D/teX Ultra1000, an electronic Si strip detector that has high dynamic range, high sensitivity, and good energy resolution, as well as not requiring any consumable gas.

Other Details:

X-ray tube:
  • Standard: Cr (Maximum load 2 kW), Effective focus size 1 × 10 mm2 (N.F.), Short type
  • Option: Cu (2 kW), Co (1.8 kW), Fe (1.5 kW), V (0.3 kW)

 

    2θ Scanning Range:
    • 2θ = 98° to 168° (Central angle range of D/teX Ultra 1000 2θc = 108° to 158°)

     

      ψ Angle Range: ψ = 0° to +60° (at maximum)

      Oscillation Range: ψp = ±1° to ±10°

      Incident Collimator: Standard: φ150 μm, φ1 mm, Option: φ30 μm, φ50 μm, φ100 μm, φ300 μm, φ500 μm, φ2 mm, φ4 mm

      Standard: Manual Z stage:
      • Lab. jack (Model LJA-16223)
      • Maximum sample space: 720 mm (W) × 560 mm (D) × 540 mm (H)
      • Stage dimensions: 160 mm × 220 mm
      • Maximum load: 30 kg

       

        Option: Auto XYZ stage:
        • Maximum sample space: 720 mm (W) × 560 mm (D) × 335 mm (H)
        • Stroke: X-Y axis = ±50 mm, Z axis = -5 mm to + 35 mm
        • Stage dimensions: 150 mm × 150 mm
        • Maximum load: 20 kg

          SoftwareResidual stress (Measurement)sin2ψ method
          Iso-inclination method, Side-inclination method
          ψ0-fixed method
          X-Y teaching function
          Residual stress (Data processing)Batch processing of multiple data
          Smoothing
          Background elimination
          LPA correction
          Kα1, Kα2 separation
          Peak search (FWHM center method, Parabolic approximation method,
          Center of gravity method, FW2/3M center method, FW2/5M center method)
          Retained austenite (Measurement)α-Fe(211): 2θ = 156.40° (Cr Kα), γ-Fe(220): 2θ = 128.83° (Cr Kα)
          X-Y teaching function
          Retained austenite (Data processing)Batch processing of multiple data
          Normalization factor of diffraction intensity: R = 0.36746 (or user setting value)


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          Rigaku SmartSite RS Stress Analyzers
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          BrandRigaku
          ModelSmartSite RS
          Dimensions114(W) x 248(D) x 111(H) mm
          Weight3 kg
          Bore Size200 mm (Diameter)
          Power SourceIntegrated Battery or AC
          Supply Voltage100-240 V
          Detector TypeHigh-Speed Two-Dimensional (2D) Semiconductor Detector

          The SmartSite RS is the world’s smallest portable stress analyzer that is especially designed for field analysis. It enables to characterize residual stress of metal parts ranging from large construction projects to individual products, e.g. bridges, maritime vessels, aircraft, aerospace equipment, pipelines, heavy machinery and automobiles.

           

          Rapid & easy data acquisition

          Residual stress is measured by 60 seconds or less in most of the cases. 1-click operation thanks to pre-define measurement and sample parameters.

           

          Remote operation through a tablet PC and Wi-Fi

          The instrument is remotely controlled by a table PC equipped with Wi-Fi communication. This design is especially useful if the measurement must be performed in a hazardous area or where access is limited.

           

          No on-site utilities required

          The integrated affords up to 100 measurements before recharging. It also doesn’t require any other utilities, like cooling water. Therefore, there is no need to prepare any special on-site utilities.

          Features:

          • The instrument is remotely controlled by a table PC equipped with Wi-Fi communication.
          • Battery operated with an exchangeable battery. There is no need to prepare utilities on-site, e.g. cooling water and electricity.
          • 1-click operation thanks to pre-define measurement and sample parameters.
          • Easy setup using integrated three-dimensional (3D) sensors and indicators displayed on table PC.
          • Easy positioning using the integrated CCD camera, LASER marker and white LED for illumination in low light environments.
          • Calibration is easily done with the included calibration standards. The calibration history is recallable at any time to ensure measurement traceability.

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